LBNL Catalysis Laboratory, UC Berkeley

Location: 20 Lewis Hall, University of California, Berkeley

                                          Contact:  Tel: (510)-643-0914

Catalysis Laboratory Manager: Cooper Citek PhD ([email protected])

For ID card access to the Catalysis Laboratory in Lewis 20, please send the following information to the Manager:

Please check the status and reservation calendars below to reserve instrument time.

Instrument	Agilent GCMS	Waters Prep HPLC-MS Autopurification System	Perkin Elmer Axion 2 TOF MS	Bruker FT-IR with MCT Detector	Shimadzu UV-Vis with Unisoku Cryostat-Stirrer	Shimadzu MALDI-TOF	Micromeritics 3Flex	Biotage Endeavor High Pressure Reactor	Mettler Toledo ReactIR Probe with EasyMax Thermostat	Viscotek GPC	Jasco J-815 CD Spectropolarimeter	CH 650E Electrochemistry Potentiostat with Inert Atmosphere	Microwave Reactor	Stopped-Flow UV-Vis-Fluorescence Spectrometer	MBraun Glovebox
Status							*Contact Superusers			*recalibrate before use				*off, restart on request
Calendar	GCMS	LCMS	TOF MS	FTIR	UV-Vis	MALDI-TOF	3 Flex	Endeavor Pressure Reactor	ReactIR	GPC	CD
SOP and Manual Documents	SOP Agilent 7890 GC Manual Agilent 7890B GC Troubleshooting	SOP MassLynx User Guide Waters Prep LCMS Autopurification Manuals Chemical Inventory	SOP Chemical Inventory AxION 2 TOF MS Users Guide AxION 2 TOF Maintenance Guide	SOP Chemical Inventory Download OPUS Viewer from Bruker	SOP	SOP Chemical Inventory - Matrices/Salts Shimadzu Axima Performance MALDI-TOF User Guide	SOP CO SOP Chemical Inventory	SOP CO SOP Biotage Endeavor User Manual	SOP	SOP	Jasco J-800 Series Software Manual	SOP CH 600E Series Potentiostat User Manual		SOP	MBraun Labmaster Manual
Superuser Contacts	Magan Powell (Rittle) [email protected] Nicodemo Ciccia (Hartwig) [email protected]	Sarah Chen (Rittle) [email protected] Chang Liu (Rittle) [email protected]	Mathew See (Tilley) [email protected] John Brunn (Hartwig) [email protected]	Alireza Pourghaderi (Maboudian) [email protected] Stuart McElhany (Maboudian) [email protected]	Alex Wheeler (Tilley) [email protected]	Tent Tangpradabkul (Schepartz) [email protected]	Kurtis Mickel Carsch  (Long) [email protected] Jesse Peltier (Long) [email protected] Rachel Rohde (Long) [email protected]	Jeremy Nicolai (Hartwig) [email protected]	Andre Sanchez (Maimone) [email protected] Alex Wheeler (Tilley) [email protected]	Nicodemo Ciccia (Hartwig) [email protected] Jake Shi (Hartwig) [email protected]	Isaac Joyner (Hartwig) [email protected]	Christina Pierson (Hartwig) [email protected] Isaac Yu (Hartwig) [email protected]		Please contact Catalysis Center Manager for permission to use.	Please contact Catalysis Center Manager for permission to use.

 Schedule

Schedule

Ion source: ESI and APCI

Columns available: Reverse phase C18 columns (both analytical and prep),

                                   Reverse phase C8 column (prep),

                                   HILIC columns (both analytical and prep).

Schedule

       Ion Source: ESI and APCI

       For HRMS, error < 5ppm

       UPLC for fast LC analysis: 18000psi

       Columns available: reverse phase C18 column

                                      Cogent Diamond Hydride column

Schedule

     Optical resolution: <0.2 cm-1

     Time resolution: Rapid Scan: 110 spec/sec; Step Scan: 10 ns.

Schedule

    The stopped-flow unit is also adapted to the FTIR spectrometer for IR kinetics.

Agilent 7890B-5977A GC-MS system     Schedule

Malvern Viscotek GPC system           Schedule

Mobile phase: THF

Molecular weight range: 1,000 – 200,000

Schedule

  8 parallel reaction vails, 2 reaction gases, up to 500 psi, 200 °C

ReactIR15 and EasyMax ChemSynthesis Station

CD Spectrometer