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Catalysis Laboratory Manager: Cooper Citek PhD

Location: 20 Lewis Hall, University of California, Berkeley

Contact: Miao Zhang, PhD, Tel: [email protected] 

                                             (510)-643-0914, Email: [email protected]

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For ID card access to the Catalysis Laboratory in Lewis 20, please send the following information to the Manager:

Please check the status and reservation calendars below to reserve instrument time.

Instrument	Agilent 7890-5977A GC-MS	Waters Prep HPLC-MS Autopurification System	Perkin Elmer Axion 2 TOF HR-MS	Bruker Vertex80 ATR-FT-IR with MCT Detector	Shimadzu UV-2600i UV-Vis with Unisoku Cryostat-Stirrer	Shimadzu Axima Performance MALDI-TOF	Micromeritics 3Flex	Biotage Endeavor High Pressure Reactor	Mettler Toledo ReactIR Probe with EasyMax Thermostat	Jasco J-815 CD Spectropolarimeter	CH 650E Electrochemistry Potentiostat in Inert Atmosphere	CEM Discover SP Microwave Reactor	Biologic µSFM Stopped-Flow UV-Vis Spectrometer	MBraun Glovebox
Status
Calendar	GCMS	LCMS	TOF MS	FTIR	UV-Vis	MALDI-TOF	3 Flex	Endeavor Pressure Reactor	ReactIR	CD
SOP and Manual Documents	SOP Agilent 7890 GC Manual Agilent 7890B GC Troubleshooting	SOP MassLynx User Guide Waters Prep LCMS Autopurification Manuals Chemical Inventory	SOP Chemical Inventory AxION 2 TOF MS Users Guide AxION 2 TOF Maintenance Guide	SOP Bruker VERTEX 80V Manual Chemical Inventory Download OPUS Viewer from Bruker	SOP	SOP Chemical Inventory - Matrices/Salts Shimadzu Axima Performance MALDI-TOF User Guide	SOP CO SOP Chemical Inventory	SOP CO SOP Biotage Endeavor User Manual	SOP ReactIR 15 Hardware Manual	Jasco815_CD_User Instructions Jasco J-800 Series Software Manual	SOP CH 600E Series Potentiostat User Manual	CEM Discover SP Microwave Reactor Manual	SOP µSFM Manual Bio-Kine32 and MOS-200M Manual	MBraun Labmaster Manual
Superuser Contacts	Magan Powell (Rittle) magan_powell Nicodemo Ciccia (Hartwig) nciccia		Mathew See (Tilley) mssee John Brunn (Hartwig) jbrunn	Alireza Pourghaderi (Maboudian) alirezapourghaderi Stuart McElhany (Maboudian) stuartm			Jesse Peltier (Long) jlpeltier Rachel Rohde (Long) rachel_rohde	Jeremy Nicolai (Hartwig) jeremy.nicolai		Isaac Joyner (Hartwig) ijoyner	Christina Pierson (Hartwig) christina_pierson Isaac Yu (Hartwig) isaacyu		Please contact Catalysis Center Manager for permission to use.	Please contact Catalysis Center Manager for permission to use.

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Ion source: ESI and APCI

Columns available: Reverse phase C18 columns (both analytical and prep),

                                   Reverse phase C8 column (prep),

                                   HILIC columns (both analytical and prep).

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       Ion Source: ESI and APCI

       For HRMS, error < 5ppm

       UPLC for fast LC analysis: 18000psi

       Columns available: reverse phase C18 column

                                      Cogent Diamond Hydride column

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     Optical resolution: <0.2 cm-1

     Time resolution: Rapid Scan: 110 spec/sec; Step Scan: 10 ns.

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    The stopped-flow unit is also adapted to the FTIR spectrometer for IR kinetics.

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Agilent 7890B-5977A GC-MS system     Schedule

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Malvern Viscotek GPC system           Schedule

Mobile phase: THF

Molecular weight range: 1,000 – 200,000

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  8 parallel reaction vails, 2 reaction gases, up to 500 psi, 200 °C

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CD Spectrometer