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A short intro into single-crystal diffraction on end-station 2 is found here:
How do I align a sample in a DAC (or generally a gasket hole) onto the beam?
How do I ensure the crystal in the DAC stays in the beam when rotating?
How do I align a crystal in air onto the X-ray beam?
How do I collect a single crystal dataset on end-station 2?
How do I laser-heat my sample in a DAC?